Guide Validation in Chemical Measurement

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Chemistry International

Automated ionselective measurement of lithium in serum A practical approach to resultlevel verification in a twoway method validation. Determination of hydrocarbons in waterinterlaboratory method validation before routine monitoring. Interlaboratory quality audit program for potable water assessment of method validation done on inductively coupled plasma atomic emission spectr A need for clearer terminology and guidance in the role of reference materials in method development and validation.

Validation of salt spray corrosion test.

5. Validation of analytical methods

Method validation and reference materials. Method validation of modern analytical techniques. Part 4 Evaluation and validation of existing systems. Analytical validation in practice at a quality control laboratory in the Japanese pharmaceutical industry. Validation of the uncertainty evaluation for the determination of metals in solid samples by atomic spectrometry.


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Validation requirements for chemical methods in quantitative analysis horses for courses? Validation design is affected by practical considerations, such as the availability of samples and their cost, the duration of the study, etc.

Additional information

Validation study may often detect imprecision, inaccuracy, requiring a return to the method development stage. Thus, it is important to understand that method validation is not a routine task. Kuselman informed the participants about method performance criteria in recently published AOAC International Guidelines. Hellmuth Broda, PerkinElmer, Switzerland, reported on novel services of his company for analytical method validation and other method lifecycle activities.

More details about the workshop and presentations in pdf format are available at http: On the two days following the conference, January, workshop participants took part in the Isranalytica Conference and Exhibition. A summary of these events is available at www.


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Fajgelj Human errors and out-of specification test results. Chem Int 35 3: Kuselman Human errors and quality of chemical analytical results. Chem Int 37 3: ISO Laboratory medicine - Requirements for reference measurement laboratories. Bettencourt da Silva, A. JCGM Guide Evaluation of measurement data—The role of measurement uncertainty in conformity assessment. Use of uncertainty information in compliance assessment, 1st ed.

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B da Siva, D. Hibbert Total risk of false decisions on conformity of multicomponent material due to measurement uncertainty abstract. Metrological and technical requirements.

Developing a Testing Plan for Medical Device Design Verification

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